简介:ARogowskicoilisdevelopedtodetectthenanosecondpulsesignalsofthedischargecurrentwithawidebandwidthof800kHzto106MHzandhighsensitivityof2.22V/A.Perfor-mancetestsshowthattheRogowskicoilhasbothexcellentdynamicandstaticcharacteristics.CalibratingresultsandthecomparisonbetweenthestandardcurrentshuntandthedevelopedRo-gowskicoilforthemeasurementofnanoseconddischargepulsesdemonstratethatthedevelopedRogowskicoilcanreproducetheactualwaveformofthedischargecurrentaccurately.
简介:Non-contactmagneticmeasurementmethodisaneffectivewaytostudytheairarcbehaviorexperimentally.Oneofthecrucialtechniquesistosolveaninverseproblemfortheelectromagneticfield.Thisstudyisdevotedtoinvestigatingdifferentalgorithmsforthiskindofinverseproblempreliminarily,includingthepreconditionedconjugategradientmethod,penaltyfunctionmethodandgeneticalgorithm.Thefeasibilityofeachalgorithmisanalyzed.Itisshownthatthepreconditionedconjugategradientmethodisvalidonlyforfewarcsegments,theestimationaccuracyofthepenaltyfunctionmethodisdependentontheinitialconditions,andtheconvergenceofgeneticalgorithmshouldbestudiedfurtherformoresegmentsinanarccurrent.
简介:Attheambienttemperatureandpressureaglowdischargeplasmawasusedasanewapproachforthecouplingofmethanewiththenewly-developedrotarymultidentatehelixelectrode.Inthepresenceofhydrogen,theeffectsoftheinputpeakvoltagesandgasflowratesonmethaneconversion,C_2singlepassyieldandselectivitywereinvestigated,andthentheresultswerecomparedwiththosefromthethree-discmultidentateelectrode.Thisdemonstrated,onanexperimentalscale,thattherotarymultidentatehelixelectrodewasbetterthanthemultidentatethree-discelectrodeastherewaslittleaccumulationofcoke,andtheC_2yieldperpasswas69.85%andC_2selectivityover99.14%with70.46%methaneconversionataninputpeakvoltageof2300Vand60ml/mingasflowrate.
简介:Aseriesofrhodium-modifiedMo-K/Al2O3catalystsampleswaspreparedbyvaryingtherhodiumloadingbetween0and1.0wt%andmaintainingmolybdenumandpotassiumcontentsasconstants.ThestructuresofthesampleswerecharaterizedbytechniquesofXRD.LRS.TPR,XPSandEXAFSandcorrelatedtothecatalyticpropertiesofthesamplesforalcoholsynthesisfromsynthesisgas,Itwasfoundthat.intheoxidicrhodium-modifiedsamples.astronginteractionoftherhodiummodifierwiththesupportedK-Mo-Ospeciesoccurs.Thisinteractionfacilitatesthesulfidationandreductionofthesupportedoxo-molybdenumandleadstoadecreaseinthesizeofthemolybdenumspeciesandstabilizationofthecationicrhodiumspeciesonthesamplesduringsulfidation.Uponsulfidation.Thesulfidedmolybdenumspeciesintherhodium-freesampleismanlypresentaslargepatechesofMoS2-likeslabswiththeirbasalsulfurplanesinteractingwiththesupportsurface.Withthemodiricationofrhodiumtothesamples.ThesupportedMoS2-likespeciesbecomeshighlydispersed.asrevealedbythedecreaseintheaveragesizeofthesulfidedmolybdenumspecies.TheinteractionoftherhodiumspecieswiththemolybdenumsomponentmaycausethebasalplanesoftheMoS2-likespeciestobecomeorientedperpendiculartothesupportsurfaceduetofavorablebondingoftheMoS2edgeplanestothesupportthroughMo-O-Albonds.Incomparisonwiththesulfidedsamplefreeofrhodium.thepropertiesoftherhodium-modifiedsamplesforalcoholsynthesisfromsynthesisgasaremuchimproved.Itmostprobablyresultsfromthesynergicinteractionoftherhodiumwiththemolybdenumspeciesthatgivesrisetotheappearanceofthecatalyticallyactivesurfacesofsites.Theco-existenceofcationicandmetallicrhodiumstabilizedbythisinteractionmayberesponsiblefortheincreasedselectivityfortheformationofC2+alcohols.