简介:通过一种取代剂将N-乙基-α-萘胺生产中副产品N,N-二乙基-α-萘胺转化产品N-乙基-α-萘胺.经试验考查了温度、时间以及反应物配比对转化反应收率的影响,确定了最佳操作条件:温度165℃,时间4小时,物料配比1:5(摩尔比).转化反应的总收率为78.4%.由于副产品N,N-二乙基-α-萘胺的转化利用,使N-乙基-α-萘胺产品收率由68.9%提高至84.3%。
简介:ThispaperpresentsadiscussiononaproblemsuggestedbyN.Salinas(J.OperatorTheory,Vol.10,1983),i.e.,ifT=(T1,T2,…,Tn)isacommutingn-tupleofhyponormaloperatorsonacomplexHilbertspace,dowehave(1)(2)δ(T-μ)=dist(μ,σl(T)),μ∈Cn?Itisprovedthattheproblems(1)and(2)arebothtrueforsomecommutingn-tuplesofsemihyponormaloperators.Ingeneralcase,problem(1)hasanegativeanswer.Asanap-plication,wepointoutthatthereexistsacommutingn-tupleofhyponormaloperatorsT(n≥2),suchthat|λ|<,whereσT(T)denotesJ.L.Taylor’sjointspectraofT,eveniftheconditionofTaylor’sjointspectraofTisgiven.
简介:2017年年初的一句“我可能复习了假书”走红后,互联网上立即涌现出一大批“假”现象,它们与传统的真假相背离,却受到社会的一致热捧。拟对“主语+可能+V了假N”进行句法和语义、语用上的考察,并分析“假”现象泛化的动态过程及其语用价值。
简介:WithN-vinyl-2-pyrrolidone(NVP)anditaconicacid(IA),poly(N-vinyl-2-pyrrolidone/itaconicacid)[P(NVP/IA)]hydrogelwassynthesizedbyfreeradicalsolutionpolymerization.ThestructureofthisP(NVP/IA)wascharacterizedbyIR.Effectsofconcentrationofitaconicacid,amountofcross-linkagent,N,N′-methylene-bis-acrylamide,reactiontemperature,andtimeonpropertiesofswellingratio(SR)ofthehydrogelwereinvestigated.Theresultsshowthatthebestswellingpropertyofthehydrogelisobtainedat50℃and1.5h.pHsensitivityincreasesastheconcentrationofitaconicacidinthehydrogelsystemincreases.Swellingratioofthehydrogeldecreasesastheamountofcross-linkagentincreases.