简介:ThemicrostructuralchangesofFe83Si4B13amorphousmotheralloyduringtheheatingprocesswereinvestigatedbyLaserScanningConfocalMicroscopy(LSCM),andthephasetransformationwasdeterminedbytheThermo-Calccalculations.ThedifferencesinthemeltingpointsmeasuredbyDifferentialScanningCalorimetry(DSC)andLSCM,andthoseobtainedbyThermo-Calccalculationswerealsodiscussed.ItisfoundthatthemeltingpointsmeasuredbyDSCandLSCMarerelativelysimilar,whereastheonsetandendofthemeltingtemperaturescalculatedbyThermo-CalcsoftwarearehigherthanthosemeasuredbyDSCandobservedbyLSCM.
简介:Themechanicalandcorrosivepropertiesof00Cr13Ni4Mo(S13-4N)weretestedandcomparedwiththoseof00Cr13Ni6Mo(S13-6).Theeffectsofnitrogenonthepropertiesofthesteelswereanalyzed.Theresultsofthetensileandcorrosiontestsshowthestrength,theductility,andthepittingcorrosionresistanceofS13-4Narehigher,lowerandpoorerthanthoseofS13-6respectively,whentemperedatatemperaturebelow550℃andviceversawhenthetemperingtemperatureishigherthan550℃.TheresultsoftheX-raydiffraction(XRD)andtheelectronbackscattereddiffraction(EBSD)analysesrevealthatinversedausteniteappearsat550℃andtheamountofitpeaksat600℃withthebestductility.AndthetotalamountoftheinversedausteniteinS13-6ismorethanthatinS13-4Nindifferentforms.Nitrogenperformsbetterintermsofstabilizinginversedaustenitewhilenickelismorefavorableforforminginversedaustenite,theamountandstabilityofwhichaffecttheductilityremarkably.ThereasonfortheembrittlementofS13-4Nat450℃canbetheresultofcarbideandnitrideprecipitatingatgrainboundaries.
简介:AhighalloyedVanadis4(V4)steelwasproducedbysprayformingprocessinBaosteel,andthemicrostructureoftheas-sprayedsteelanditsevolutionduringhotrollingandannealingprocesseswerecharacterized.Itwasfoundthattheas-sprayedV4steelhasahomogeneousandfinescalemicrostructurewithuniformdispersionofcarbides.Thehotrollingtemperatureisthekeyfactorincontrollingtheevolutionoftype,morphologyanddistributionofcarbides,aswellasthematrixmicrostructureoftheas-rolledsteels.Theoptimizedprocessingparametersfortheas-sprayedV4steelarerollingat1050℃andthenannealingat900℃.Themicrostructuralevolutionmechanismsduringhotrollingandannealingaredeterminedaccordingtothemicrostructuralanalyasisofthematerialatdifferentstages.