简介：Thecoordinationpolymer,(Nd(H2O)5)2(2,6-AQDS)3·2H2Owhere2,6-AQDS=2,6-anthraquinonedisulfonate,hasbeensynthesisedviaahydrothermalroute.Structurally,itconsistsoflayersofmonomericNdpolyhedrawhicharelinkedby2,6-AQDSanionsformingapolymeric,three-dimensionalnetwork.EachNdatomisninecoordinate,bondingtofivewatermoleculesandtofouroxygenatomsfromfour2,6-AQDSanionswhichinturnpillarthelayersbybridgingtwoNdatomsinonelayer,andcoordinatingtoasingleNdintheother.

简介：NanocrystallineSnO2wassynthesizedbydirectmixingandgrindingofSnCI4-5H2OandNaOHatroomtemperature,followedbycalcinationatdifferenttemperaturesfordifferenttimesinair.ProductsampleswerecharacterizedbyX-raydiffractionandtransmissionelectronmicroscope,revealingthattheamorphousprecursorSnO2wastransformedtocrystalsat200℃for3h,andthattheaverageparticlesizeincreaseduponraisingthecalciningtemperatureorprolongingthecalciningtime.Themechanismofthephasetransformationoftheproductsisdiscussed.

简介：连贯的多角形的粒子的二维的分离元素模型(DEM)模拟被开发了估计点来源颤动的利益在楔形的hoppers导致流动。使用的particleparticle相互作用模型基于一个多接触原则。没有颤动，学习的第一部分在严肃下面调查了粒子分泌物决定批评的孔尺寸(Bc)就作为粒子形状的功能支撑流动。多角形形状的粒子比圆形的粒子需要一个更大的孔，这被显示出。当粒子顶点的数字增加，Bc减少，这也被显示出当粒子顶点的数字增加。圆形的粒子的增加以一种线性方式支持多角形的流动。学习的第二部分证明那颤动能提高流动，有效地减少Bc。模型表明了震荡器地点(高度)的重要性，与在提高的以前的连续统模型结果，和颤动振幅一致流动。

简介：Uniformlysizedα-Fe2O3hexagonalplateletsweresynthesizedbyahydrothermalprocessusingFe(OH)3suspensionandlargeamountofNaOH.ThereactionproductswerecharacterizedbyX-raydiffraction(XRD),scanningelectronmicroscopy(SEM),transmissionelectronmicroscopy(TEM),selectedareaelectrondiffraction(SAED),andavibratingsamplemagnetometer(VSM).Theresultsshowthatthehexagonalplateletsarefine,monodisperseandconsistingofsingle-crystals.Themagnetichysteresis(M-H)curveofthesamplesmeasuredatroomtemperatureindicatesthattheα-Fe2O3micro-plateletsexhibitferromagneticbehaviorswithrelativelylowcoercivity.

简介：Commerciallyavailablelatticescontainvariouskindsofmorphologicalimperfectionswhichresultingreatdegradationinlattices’mechanicalproperties,therefore,toobtainimperfectioninsensitivelatticestructureisobviouslyapracticalresearchsubject.Hierarchicalstructurematerialswerefoundtobeaclassofpromisinganti-defectmaterials.Thispaperbuildshierarchicallatticebyaddingsoftadhesiontolattice’scelledgesandnumericalresultsshowthatitsimperfectionsensitivitytomissingbarsisminorcomparedwiththeclassiclattice.Softadhesionwithappropriatepropertiesreinforcecelledge’sbendingstiffnessandthusreducethebendingdeformationinlatticecausedbymissingbarsdefect,whichisconfirmedbystatisticalanalysisofnormalizednodedisplacementsofimperfectlatticesunderhydrostaticcompressionandshearloads.

简介：Inthisarticle,low-pressurecontrolmethodsforacombinedarcsubmergednanoparticlesynthesissystem(ASNSS)wasproposedanddevelopedforTiO2nanoparticlefabrication.Thephotocatalyticreactioniscarriedoutinaphotochemicalreactor.TheUVlightisobtainedfromUV-lampswithwavelengthof(253.7±0.8)nm.TheUV-Visspectrometryisusedtomonitortheabsorbancespectraofmethyleneblueasafunctionofilluminationtime.ExperimentalresultsshowthattherateconstantofphotocatalyticreactionofTiO2nanoparticlesformethyleneblueis0.0365min^-1.Thesurfaceadsorptionplaysanimportantroleinthedecompositionofmethyleneblue.ExperimentalresultsindicatethattheTiO2nanoparticlefluidpossessesexcellentphotocatalyticactivityinphotodegradationofmethyleneblue.

简介：Thereisaneedtostandardizemethodsassociatedwiththedispersionofnanomaterialsinnano（eco）toxicologicalinvestigations.Thefirststeptowardthisgoalistounderstandthedegreeofvariabilitythatexistsinnanomaterialdispersionspreparedbyusingdifferentprotocols.Usingtwocasestudies,thedegreeofvariabilityinTiO2nanomaterialdispersionswasassessedbydifferentialcentrifugalsedimentation（DCS）methods.Casestudy1addressesthevariabilitythatarisesfromvariationswithinoneprotocol,investigatingtheeffectsofdispersionaging,sonicationexposuretime,sonicationinthepresence/absenceofanicebath,materialsubsampling,particleconcentrationandhavingapre-wettingstep.Casestudy2addressesthevariabilitybetweenfourdifferentprotocolsdevelopedthroughpastresearchactivitiesandprojects.Theresultsindicatethatthereisalargedegreeofvariability（relativestandarddeviation（RSD）ofmeanparticlediameter=26%）inthedispersionofTiO2nanomaterialsbetweenthefourdifferentprotocolsstudiedandthatseveralstepsinadispersionprotocolarepotentialsourcesofvariation,withfinalparticleconcentrationbeingthemostsignificant.Theimplicationofthisstudyisclear:forthepurposeofdatacomparability,thereisaneedtoprovidetheexactdetailsofallstepsinvolvedinadispersionprotocol.

简介：为nanostructuredSnO2的先锋在不同条件下面经由一个帮助微波的热水的方法被综合，用SnCl2吗？

简介：Laminatedcompositematerialsarewidelyimplementedinseveralengineeringconstructions.Foritsrelativelightweight,thesematerialsaresuitableforaerospace,military,marine,andautomotivestructuralapplications.Toobtainsafeandeconomicalstructures,themodellinganalysisaccuracyishighlyrelevant.Sincemeshlessmethodsintherecentyearsachievedaremarkableprogressincomputationalmechanics,thepresentworkusesoneofthemostflexibleandstableinterpolationmeshlesstechniqueavailableintheliterature—theRadialPointInterpolationMethod(RPIM).Here,a2Dapproachisconsideredtonumericallyanalysecompositelaminatedbeams.Boththemeshlessformulationandtheequilibriumequationsrulingthestudiedphysicalphenomenonarepresentedwithdetail.Severalbenchmarkbeamexamplesarestudiedandtheresultsarecomparedwithexactsolutionsavailableintheliteratureandtheresultsobtainedfromacommercialfiniteelementsoftware.Theresultsshowtheefficiencyandaccuracyoftheproposednumerictechnique.

简介：在组成的部件之间的有瑕疵的结合能极大地影响合成结构的性质。处于2Dfibrereinforced的问题产生的有瑕疵的接口的不同类型的asymptotic分析合成材料被建议。执行学习基于管理biharmonic问题的asymptotic减小进二个泛音问题。所有答案在一种关上的分析形式被获得。获得的结果能被用于撤退和pushout测试的计算，以及为合成材料的破裂的调查。

简介：ThecaptureoforthophosphatesandtotalphosphorusfromthePudongCanalriverinthePudongDistrictofShanghaibyTiO2nanoparticlesisstudiedusingarotatingphotoreactorandthenano-TiO2photocatalystDegussaP25.TheeffectsofUVirradiationintensityinarangeof20-74mW/cm2.theloadingoftheTiO2nanoparticlesinarangeof0.05-0.1g/L,irradiationtimeupto4h,andpHvaluesinarangeof2-10.5onthecaptureefficiencyareinvestigated.TheresultsshowthatthecaptureoforthophosphatesandtotalParesignificantlyenhancedbyUVirradiation;ataloadingof0.1g/Landanirradiationintensityabove36mW/cm2,orthophosphatesandtotalphosphorusarerapidlycapturedbyTiO2nanoparticles,causinganobservedreductionfrom0.4mg/Ldownto0.02mg/L.pHvaluesinarangeof2-10.5havelittleeffectonthecaptureefficiencyoforthophosphatesandtotalphosphorus.

简介：Hierarchicalsea-urchin-shapedmanganeseoxidemicrospheresweresynthesizedviaatacilemetnoabasedonthereactionbetweenKMnO4andMnSO4inHNO3solutionat50C.Theaveragediameterofthemicrospheresis850nm.Themicrospheresconsistofacoreofdiameterof800nmandnanorodsofwidth50nm.Thenanorodsexistattheedgeofthecore.TheBrunauer-Emmett-Tellersurfaceareaofthesea-urchin-shapedmicrospheresis259.4m2/g.Apossibleformationmechanismofthehierarchicalsea-urchin-shapedmicrospheresisproposed.Thetemperaturefor90%conversionofbenzene(T90%)onthehierarchicalurchin-shapedMnO2microspheresisabout218℃.

简介：

简介：ZrO2nanopowdersbasedstearicacidphasechangematerials(PCMs)werepreparedbyhigh-energymilling.Theconceptofheatcapacityfactor(HCF)wasusedtoanalyzethethermalpropertiesofthematerials.TheheatstoragepropertyofPCMs,containingthesamecontentofstearicacid(23%bymass)inthestartingmaterialsbutsynthesizedbydifferenttechnicalprocesses,wasinvestigatedbyusingHCF.Itwasfoundthattherewerevastinfluencesofdifferentdispersantsontheheatcapacity.Thesamplespreparedwithchloroformprovidedthebestheatstorageabilityinallsamplestested.

简介：Anewmicromechanicsconstitutivemodelforpuredilatanttransformationplasticityofstructureceramicsisproposedinthispaper.Basedonthethermodynamics,micromechanicsandmicroscalet→mtrans-formationmechanismanalysisoftheTZPandPSZZrO2-containingceramics,ananalyticexpressionsoftheHelmholtzandcomplementaryfreeenergyoftheconstitutiveelementforthecaseofpuredilatanttransforma-tionisderivedforthefirsttimeinaself-consistentmanner.Bytheanalysisofenergydissipationinthefor-wardandreversetransformations,themieromechanicsconstitutivelawisderivedintheframeworkofHill-Rice’sinternalvariableconstitutivetheory.

简介：Afacilemethodforthesynthesisofsilver-silica（Ag-SiO2）Janusparticleswithfunctionalitiessuitablefortextileapplicationsisreported.SilicananoparticlespreparedbytheStobermethodwerefunctionalizedwithepoxy,amine,andthiolgroups,whichwereconfirmedbyFouriertransforminfraredanalysis.ThefunctionalizedsilicananoparticleswereusedtoproducePickeringemulsions,andtheexposedsurfacewasusedfortheattachmentofsilvernanoparticles（AgNPs）viathelow-temperaturechemicalreductionmethod.ThemorphologyandstructureoftheAg-SiO2Janusparticleswerecharacterizedbyscanningelectronmicroscopy,scanningtransmissionelectronmicroscopy,high-resolutiontransmissionelectronmicroscopy,energy-dispersiveX-rayanalysis,andUV-visspectroscopy.Becauseoftheirspecificfunctionalities,theseAg-SiO2Janusparticlesareproposedforapplicationsontextilesubstrates,astheycanovercomeseveraldrawbacksofdirectapplicationofAgNPsontextiles,suchasleaching,agglomeration,andinstabilityduringstorage.

简介：Thispaperpresentsanovelmechanicalattachment,i.e.,nonlinearenergysink(NES),forsuppressingthelimitcycleoscillation(LCO)ofanairfoil.Thedynamicresponsesofatwo-degree-of-freedom(2-DOF)airfoilcoupledwithanNESarestudiedwiththeharmonicbalancemethod.DiferentstructureparametersoftheNES,i.e.,massratiobetweentheNESandairfoil,NESofset,NESdamping,andnonlinearstifnessintheNES,arechosenforstudyingtheefectoftheLCOsuppressiononanaeroelasticsystemwithasupercriticalHopfbifurcationorsubcriticalHopfbifurcation,respectively.TheresultsshowthatthestructuralparametersoftheNEShavediferentinfluenceonthesupercriticalHopfbifurcationsystemandthesubcriticalHopfbifurcationsystem.

简介：为它的高氧化抵抗，钇硅酸盐是为在在1600°C上面的温度的carbon-fiber-reinforcedcomposites的保护的涂层的一个重要候选人。一个新奇方法，由一起沉淀组成，弄干水花，热处理和plasma-densification，被开发准备Y2SiO5粉末为热喷洒。作文，形态学和综合Y2SiO5粉末的流动能力被XRD，SEM和霍尔流量计分别地调查。结果证明综合Y2SiO5粉末与高纯净是将近球形的。分别地，Y2SiO5粉末的明显的密度和流动能力是1.87g/cm3和37s/50g它为大气的血浆喷洒导致多达80%的高免职效率。

简介：Aunifiedperturbationtheoryisdevelopedhereforcalculatingsolitarywavesofallheightsbyseriesexpansionofbaseflowvariablesinpowersofasmallbaseparametertoeighteenthorderfortheone-parameterfamilyofsolutionsinexactform,withallthecoefficientsdeterminedinrationalnumbers.Comparativestudiesarepursuedtoinvestigatetheeffectsduetochangesofbaseparameterson(i)theaccuracyofthetheoreticallypredictedwavepropertiesand(ii)therateofconvergenceofperturbationexpansion.Twoimportantresultsarefoundbycomparisonsbetweenthetheoreticalpredictionsbasedonasetofparametersseparatelyadoptedforexpansioninturn.First,theaccuracyandtheconvergenceoftheperturbationexpansions,appraisedversustheexactsolutionprovidedbyanearlierpaper[1]asthestandardreference,arefoundtodepend,quitesensitively,onchangesinbaseparameter.Theresultingvariationsinthesolutionarephysicallydisplayedinvariouswavepropertieswithdifferencesfounddependentonwhichproperty(e.g.thewaveamplitude,speed,itsprofile,excessmass,momentum,andenergy),onwhatrangeinvalueofthebase,andontherankoftheordernintheexpansionbeingaddressed.Secondly,regardingconvergence,thepresentperturbationseriesisfounddefinitelyasymptoticinnature,withtherelativeerrorδ(n)(therelativemean-squaredifferencebetweensuccessiveordersnofwaveelevations)reachingaminimum,δm,ataspecificorder,n=nm,bothdependingonthebaseadopted,e.g.n=11-12basedonparameterα(waveamplitude),nm,β=15onβ(amplitude-speedsquareratio),andnm.∈=17on∈(wavenumbersquared).Theasymptoticrangeisbroughttocompletionbythehighestorderofn=18reachedinthiswork.

简介：Nano-sizedhexagonalmagnesiumhydroxide（Mg（OH）2）withgooddispersibilitywassynthesizedbyadoubleinjection-hydrothermalmethod,utilizingpolyvinylpyrrolidone（PVP）asanadditiveandwithoptimizedprocessingparameters.SEMandBETanalysisshowedthatthemeanparticlesizeandspecificsurfaceareaoftheMg（OH）2particleswere174nmand50.77m2/g,respectively.TheFT-IRspectraandtheXRDpatternsshowedthatPVPwasadsorbedonthesurfaceoftheMg（OH）2crystal,thuseffectivelylimitingparticleagglomerationandhinderingcrystalgrowthalongthe（101）plane.TGAshowedadecreaseinthedecompositiontemperatureandanincreaseintheweightlossoftheMg（OH）2particlesduetoadditionofPVP.