简介:选取三江平原典型沼泽湿地——毛苔草沼泽,通过人工施加氮肥和磷肥来模拟农田污水排入沼泽湿地后,沼泽植物对污水的净化效果。从植物营养吸收角度进行野外实地污水净化模拟研究,对植物直接吸收利用的营养成分NH4^+-N、PO4^3--P进行了测试分析。研究表明毛苔草沼泽对水中的NH4^+-N、PO4^3--P的净化随时间的推移呈现明显的指数衰减下降趋势,随着氮、磷含量的增加,沼泽湿地对污水净化逐渐变慢,净化所需时间增长,曲线数值方程模拟效果较好。
简介:测定无机化工产品中的N(NH^+4)、Cl的含量,若将甲醛法和莫尔法相结合,则有以下特点:(1)快速经济,分析条件易于控制;(2)实现了NH^+4的分析和掩蔽一次完成;(3)有较好的精密度和准确度,可以在一定范围内进行试用。
简介:设D是无平方因子正整数.本文证明了:当D不能被形如6k+1之形素数整除时,方程,-1=Dyn仅当D=17时有正整数解(x,y,n)=(18,7,3)适合n>2.
简介:Si3N4/TiCnanocompositeceramicshavebeenfabricatedbyhotpressingtechniquewithAl2O3andY2O3asadditives.TheresultsshowedthatwelldispersedcompositepowderwascarriedoutbyaddingdispersantandadjustingpHvaluesofsuspensions.RemarkableincreaseinflexuralstrengthatroomtemperatureswasobtainedbyaddingnanoparticlesinSi3N4matrixwith10%(wtpct)ofnano-Si3N4and15%ofnano-TiC.Theflexuralstrength,fracturetoughnessandhardnesswere1025MPa,7.5MPa·1/2and15.6GPa,respectively.Themicrostructuresofmaterialswereanalyzedbyscanningelectronmicroscopy(SEM)andtransmissionelectronmicroscopy(TEM),whichindicatedthatTiCnanoparticlesdistributeinthematrixandatthegrainboundaries.Accordingtothefractureform,lowcontentsofnanoparticlescouldrefinematrixgrainsandleadtothecrackdeflectionaswellascrackpinning.Themultiplexmicrostructurewasformedbymixingnano-Si3N4particles.Thecracktrajectoriesexhibitedcrackdeflection,rod-likegrainbridgingandpull-out.
简介:目的探讨化疗加放疗治疗N2、N3期鼻咽癌的价值。方法90例N2、N3期鼻咽癌随机分为放疗化疗组(放化组)和单纯放疗组(单放组)。结果放疗化疗疗组和单纯放疗组近期鼻咽部肿瘤完全消退率分别为91.8%和84.0%(P〈0.05);两组颈部淋巴结转移灶完全消退率为83.8%和64.9%(P〈0.05)。两组3、5年鼻咽部肿瘤控制率分别68.3%和43.6%(P〈0.05),54.8%和36.1%(P〈0.05);两组颈部淋巴结转移灶控制率分别是64.7%和40.90k(P〈0.05),54.1%和35.2%(P〈0.05):两组3、5年的远处转移率分别是19.9%和42.9%(P〈0.05),28.9%和48.9%(P〈0.05);两组3、5生存率分别是56.7%和32.9%(P〈0.05),45.5%和25.9%(P〈0.05)。放疗化疗组的消化道反应、血液毒性均高于单纯放疗组(P〈0.05),但病人可以耐受。结论同步放化疗治疗N2、N3期鼻咽癌有助于提高生存率,减少局部复发和远处转移。
简介:Si3N4powderandhot-pressedSi3N4ceramicsaddedwithAl2O3areusedforinvestigatetheiroxidationbehviorinairandnitrogenatmosphere(withoxygenpartialpressurePO2=1-10Pa),TheoxidationproductsofSi3N4areexaminedbychemicalanalysi,X-raydiffraction(XRD)andXPSmethod,Also,thermodynamiccalculationismadetoanalyzeoxidationbehaviorofSi3N4.TheresultsshowthatonlypassiveoxidationwilloccurwhenSi3N4isoxidizedinairathightemperature,whereasinN2athightemperature,theactiveoxidationisdominantinspiteoftheexistenceofalittlepassiveoxidation.
简介:ThemechanicalpropertiesofpressurelesssinteringFe-Si3N4bondedSiCandSi3N4bondedSiCwithsamemanufactureprocesshavebeencomparedinthispaper.TheoxidizingmechanismofFe-Si3N4bondedSiCceramicmatrixcompositehasbeeninvestigatedespeciallythroughTG-DSC(thermogravimetricanalysis-differentialscanningcalorimeter)experiment.DuringoxidationprocedurethemainreactionistheoxidationofSiCandSi3N4,SiO2whichformprotectingfilmtopreventfurtheroxidizing.AndresidualironinthesamplesbecomeFe2O3andFe3O4,theoxidationkineticsat1100~1300℃ofre-Si3N4bondedSiChasbeenstudiedespecially.Theweightgainperunitareaatinitialstagechangesaccordingtobeelinerule,inthemiddleaccordingtoconic,andinthelastoxidationperiodfollowsparabolarule.
简介:Thetetranuclearalkyltin(Ⅳ)compounds{[R2Sn(C9H8N3O3)O]SnR3}2[R=n-Bu(1),4-CNC6H4CH2(2),C6H5CH2(3),4-ClC6H4CH2(4)]werepreparedbythereactionofSchiffbaseligandpyruvicacidisonicotinylhydrazonewith(R3Sn)2Ointhecorrespondingmolarratioof1:1.Allcompoundshavebeencharacterizedbyelementalanalysis,IRand^1HNMRspectra.Thecrystalstructureofcompound1wasdeterminedbyX-raysinglecrystaldiffractionalanalysis.Thiscompoundexhibitsadimericstructurecontainingdistannoxaneunitswithtwotypesofthetinatoms.Forthefirsttinatom,itappearstobeseven-coordinatedwithadistortedpentagonalbipyramidgeometry,andtheotherisfive-coordinatedwithadistortedtrigonalbipyramidalgeometry.Themoleculesarepackedintheunitcellintwo-dimensionalnetworkstructurethroughaninteractionbetweentheNatomsofthepyridineandthetinatomsofanadjacentmolecule.
简介:4个欧洲国家将获得第一批366架战术运输和海军护卫舰直升机,这是欧洲缔结的最大防御交易之一。来自意大利、德国、法国和荷兰的国防与武器负责人签署了一项政府间的协议,向NH工业公司购买295架NH—90,价植63亿美元,加上购买选择权,这次交易价值85.9亿美元。仍然要签订的合同是制造工具和所有设备,还有打算为德国制造的搜索与救援型的15套全套部件。