简介:通过金相显微镜(OM)、扫描电镜(SEM)和动态热机械分析仪(DMAQ800)等分析手段研究粉末冶金法制备的Ti-47Al-2Cr-2Nb-0.2W(原子分数,%)合金微观组织对其阻尼性能的影响。研究结果表明:Ti-47Al-2Cr-2Nb-0.2W合金初始组织为近γ组织,其阻尼性能最差,在振幅为100μm时,损耗因子仅为0.007;在1330℃下保温15min空冷可获得细小全层片组织,层片晶团的平均尺寸约为200μm,其损耗因子在振幅为100μm时达到0.012。随温度升高或保温时间延长,层片尺寸和晶团尺寸明显增大,合金阻尼性能下降,保温120min时层片晶团的平均尺寸约为510μm,其损耗因子在振幅为100μm时为0.009。细小全层片的阻尼性能最好,而双态组织的阻尼性能介于近γ组织和细小全层片组织之间。
简介:在80%Al-20%CuO(质量分数)体系中,通过原位反应法制备Al2O3p-Al复合材料。采用不同方法研究CuO颗粒粒度对复合材料合成温度和显微组织的影响。结果表明,CuO颗粒粒度对Al-CuO体系的完全反应温度有显著影响:含有粒度小于6μmCuO颗粒样品的完全反应温度比含有粒度小于100μmCuO颗粒样品的完全反应温度低200°C。当反应温度低于某一临界值时,原位Al2O3颗粒和Al基体之间不能完全结合;当温度高于某一临界值时,原位Al2O3颗粒的形貌从棒状转变成近球形。这两个临界温度受CuO颗粒粒度的影响:含有粒度小于6μmCuO颗粒样品的临界温度比含有小于100μmCuO颗粒样品的临界温度低100℃。
简介:Duetolowactivationcharacteristics,desirablehigh-temperaturestrength,goodresistancetoradiationdamageandusablefabricationproperties,vanadium(V)alloysareattractivecandidatestructuralmaterialsforfusionreactors[1].Irradiationinducedhardening/embrittlementatlowtemperatureisamajorproblemforthematerialsapplicationinfusionreactor[2].Inthisstudy,H/Heionswithvariousenergieswereusedtoirradiateapurevanadium(V)andaValloy(V-4Ti)toobtainadamageplateaufromsamplesurfacetothedepthof1.5m,asshowninFig.1[3].Thedetailsofirradiationparameters(energies,fluences)forHandHeionsareshowninTable1.NanoindentationwasperformedtoinvestigatethehardeningbehaviorofV-4TialloyandpureVunderirradiation.
简介:基于ABAQUS/Explicit对Ti-15-3钛合金室温锥杯成形实验中悬空侧壁起皱现象进行分析,通过对零件边缘的皱纹波长和峰高的定量研究,获取较适合Ti-15-3钛合金室温成形侧壁起皱的模拟参数。将Ti-15—3钛合金室温锥杯成形起皱获取的模拟参数,用于Ti-15-3钛合金凸弯边橡皮成形起皱的预测,通过定量比较凸弯边边缘的皱纹波长和峰高,分析不同硬度的橡皮对Ti-15-3钛合金凸弯边橡皮成形起皱的影响。经实验验证,有限元模拟对Ti-15—3钛合金凸弯边上皱纹的模拟与实验结果有很好的一致性。
简介:钛酸铝系复合材料中钛酸铝的体积分数不同,会导致Al2TiO5/Al2O3复合材料的抗铝液浸渗性能的不同。在Al2TiO5中分别按10%、20%、40%、60%、80%、90%(体积分数)引入Al2O3进行复合。通过对渗铝试样的外观形貌、微观结构分析,进而对其铝液浸渗性能进行了分析比较,发现富钛酸铝的钛酸铝/氧化铝复合材料(妒(AL2TiO5)〉40%)抗铝液浸渗性能好;而富氧化铝的钛酸铝/氧化铝复合材料(φ(Al2TiO5)〈20%)有金属铝液沿热震产生的裂纹渗入复合材料内部,容易导致复合材料断裂失效。该研究结果对可靠应用钛酸铝系复合材料作为铝液的容器具有实际工程应用价值。
简介:采用机械合金方法制备Al—V—Fe纳米晶合金粉末,合金粉末由纳米尺度的铝晶粒加非晶颗粒组成。利用Mossbauer测定表明合金由单铁组态、双铁组态固溶体以及非晶相组成,三者的含量分别为22.644%,16.746%,60.610%。
简介:以浸渍法制备的10%V/Al2O3为催化剂,研究对GB染毒空气的脱除效果,考察接触时间、温度、温度和浓度等因素对GB染毒空气脱除效果的影响,用GC-MS和LC-MS对尾气组分进行了检测分析.
简介:CuO/γ-Al2O3catalystswerepreparedbyplasmatreatmentandconventionalimpregnationmethods.Thecatalyticcombustionoftwokindsofvolatileorganiccompounds(VOCs),tolueneandbenzene,werecarriedoutovertheseCuO/γ-Al2O3catalysts.ThesurfacepropertiesofthesecatalystswerecharacterizedbyX-rayDiffraction(XRD)andScanningElectronMicroscopy(SEM).TheexperimentalresultsshowedthatincatalyticcombustiontheactivityoftheCuO/γ-Al2O3catalystpreparedviaplasmawasmuchhigherthanthatoftheCuO/γ-Al2O3catalystpreparedbyconventionalimpregnationmethod.XRDresultsshowedthatanenhanceddispersionhadbeenachievedwiththeplasmatreatment.SEMresultsindicatedthatthesizebecamemuchsmallerandthesurfacebecamemoreuniformwiththeplasmatreatment.
简介:Researchonnewtypesofcastables,pre-castassemblypartsandthermalinsulationmaterialswithgoodresistancetowear,thermalshockanderosion,andlowthermalconductivity,wasdonetosolveproblemsofhighsystemenergyconsumption,crackingandspallingofpartialliningandmismatchoffurnacetopmaterialandhangingmaterialandsoon,causedbyunreasonabledesignofChina'sAl(OH)3dilutephasefluidizedbedroastingfurnacelining.Severaldifficultproblemssuchasthematchingofdifferentmaterials,preservationofexpansionjointsamongdifferentzonesandreasonablemechanicaldistributionofliningweresolved.'Integratedfurnace'conceptwasestablishedincludingrefractoriesR&D,liningstructuredesign,constructionoptimization,furnacewarmingtechnology,initialoperationandliningmaintenancetechnology.Thekeytechnologiesofhigh-efficiencyandenergy-savingforfurnacesweredeveloped.TheseachievementshavebeenappliedtoChina'sAl(OH)3dilutephasefluidizedbedroastingfurnacestoreduceenergyconsumptionby1000MJpertonalumina,enhancethecapacityandreducetheexhaustgasemission.
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简介:从同样渗出的镁合金Mg-3%Al-1%Zn(AZ31)营舍准备的样品在低周期的疲劳测试被利用以便调查频率依赖者疲劳生活。充分颠倒的控制紧张的紧张压缩疲劳测试在空中在1Hz和10Hz的频率被执行。微观结构被光显微镜学(OM)和扫描电子显微镜学(SEM)检验。当紧张振幅比0.2%低时,疲劳生活与装载频率展出了积极关联,并且twinning的活动在10Hz被增加。当紧张振幅比0.2%高时,重要twinning在生活被发现独立于频率的这二频率,和疲劳被观察。为这频率相关的疲劳一生的可能的原因可能由于在装载频率和紧张振幅之上的twinning的依赖。
简介:Inordertoimprovetheservicelifeofcorundumliningforinductionfurnace,corundumdryrammingmixwaspreparedusingbrowncorundum,fusedmagnesia,andα-Al2O3micropowderasmainstartingmaterials,andtheinfluenceofα-Al2O3micropowderadditions(0,1%,2%,and3%,inmass)onpropertiesofcorundumdryrammingmixwasinvestigated.Theresultsshowthatafterheattreatingat1600℃,withtheincreaseofα-Al2O3addition,thepermanentchangeindimensionsonheatingofthespecimensdecreasesfirstlyandthenincreases,bulkdensityincreases,apparentporositydecreases,andthecrushingstrengthdeclinesfirstlyandthenenhances;whentheadditionofα-Al2O3is2mass%,thepermanentchangeindimensionsonheatingofthespecimensisrelativelysmallandthecrushingstrengthdecreasesto22.8MPa.TheXRDandSEMresultsshowthatafterfiringat1600℃for3hsmallgranularmagnesiumaluminatespinelformsandiswelldistributed,whichenhancesthedensity.