简介:反应粉末水泥(RPC)的三种类型的影响行为用测试方法的裂口Hopkinson出版社酒吧(SHPB)被学习。这些RPC分别地与0%,3%,和4%的钢纤维体积部分被准备。压力紧张关系,紧张率敏感阀值价值,动态力量增加因素,弹性的模量和使遭到影响负担的这些RPC标本的失败模式被调查。从测试,50s1的紧张率敏感阀值价值被获得。试验性的结果看了那紧张率什么时候从阀值价值增加了到RPC的最大的压力增加了大约20%的95s1,,RPC的弹性的模量增加了大约30%。当使遭到了影响时,有钢纤维加强的RPC标本的失败模式与RPC矩阵标本的很不同装载。在装载率的类似的影响下面,在钢纤维开发的裂缝增强了RPC标本,虽然RPC矩阵标本被分解为小片。
简介:Anovelmethodforpreparationofpolymer-basedmagneticmicrosphereswasproposedbyutilizingmeltreactiveblending,whichwasbasedonselectivelocationofFe_3O_4nanoparticlesinPA6domainsofpolystyrene(PS)/polyamide6(PA6)immiscibleblends.ThemorphologyofPA6/Fe_3O_4compositemagneticmicrosphereswasstudiedbyscanningelectronicmicroscopy(SEM).Thecompositemagneticmicrospheresweresphericalwithadiameterrangeof0.5-8μm;thediameterwassharplydecreasedwithaverynarrowdistributionbyaddingterminalmaleicanhydridefunctionalizedpolystyrenes(FPS)forreactiveblending.Transmissionelectronmicroscopy(TEM)andthermogravimetryanalysis(TGA)resultsshowedthatmostofFe_3O_4waslocatedinthePA6microspheres.MagnetizationdatarevealedthemagnetitecontentofPA6/Fe_3O_4microsphereswasabout32wt%andthesaturationmagnetizationcouldbeupto17.2Am~2/kg.
简介:LeachingexperimentsonmetakaolinshowthatthefinalAlextractionratioreachedinabatchreactionisstrikinglyinfluencedbytheinferiorporestructuregeometryofthemetakaolinpellets.Bycalciningkaolinparticlesadheredinlowhumiditystate,avarietyofmetakaolinpellet,insidewhichalargeopeningsstructuredeveloped,hasbeenprepared.Thestructureremarkablybenefitsleachantiontransference,so,thevarietyhashighacidleachingreactivity,evencoarseasthepelletsare,itsaluminumextractedratiostillhasalinearrelationshipwithleachingtime,andtheleachingkineticsismaintainedzeroorderuptoasignificantconversiondegree.ArevisedPellet-ParticleModelhasbeendevelopedtointerpretthestructureinfluenceonAlextractionratio.
简介:PolycrystallineZnOfilmswerepreparedonglasswaferusingZntargetsbyradiofrequency(RF)reactivesputteringtechniqueunderdifferentdepositionconditions.X-raydiffraction(XRD)andopticaltransmittancespectrumwereemployedtoanalyzethestructureandopticalcharacterofthefilms.Thestrainandstressinfilms,aswellasthepackingdensityarecalculatedintermsofrefractiveindexoffilmsmeasuredwithanellipticpolarizationanalyzer.ItisthedepositionconditionsthathavegreateffectsonthestructuralandopticalpropertiesofZnOfilms.Undertheoptimalconditions,theonlyevidentpeakinXRDspectrumwas(002)peakwiththefullwidthathalfmaximum(FWHM)of0.20°showingthegrainsizeof42.8nm.Thepackingdensity,thestressin(002)planeandtheaverageopticaltransmittanceinthevisibleregionwereabout97%,-1.06×109N/m2and92%,respectively.
简介:Thispaperdescribesthepreparationofpolystyrylsulfonylchloride,areactiveintermediate,anditsapplicationinsynthesesoffunctionalizedpolymerswhichcanbeusedinorganicchemistryaspolymericreagents,supportsandincontrolledreleasesystems.
简介:BackgroundTheprognosticvalueofserumC-reactiveprotein(CRP)inpatientswithinfectiveendocarditis(IE)isnotwellelucidated.ThisstudyaimedtoevaluatetheusefulnessofCRPinpredictingtheoutcomeofIE.MethodsTwohundredninty-sixpatientsfrom2009to2012intheDepartmentofCardiologyatGuangdongGeneralHospitalwerescreenedanddividedintosurgicalandconventionaltreatmentgroups.CRP,whitebloodcell(WBC),erythrocytesedimentationrate(ESR)andotherclinicaldatawereobtainedwithfollow-upfor12months.ResultsTwohundredthirty-sixpatientswereassignedtoreceivesurgerytreatmentwhile60patientsreceivedconventionaltreatment.Inthesurgerygroup,thelevelofCRPinthedeathpatientswassignificantlyhigherthanthatinthesurvivalpatients(P<0.001).TheareaunderthecurveofROCwasabout0.749(SE0.064,P=0.005,95%CI,0.624-0.874)andthecut-offpointofCRPwas23.8mg/L.Inconventionalgroup,therewassignificantdifferencebetweendeathandsurvival(P<0.001).TheareaunderthecurveofROCwasabout0.701(SE0.095,P=0.032,95%CI,0.515-0.888)andthecut-offpointsofCRPwas65.6mg/L.TherewerenosignificantdifferencesinWBCandESRbetweensurgeryandconventionalgroups.ConclusionAmoreaggressivesurgicalinterventionresultsinabetteroutcomeoverconventionaltreatmentandCRPcouldbeservedasapredictivemarkerforadverseoutcomeinIEpatients.
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简介:Anactiveandreactivecombinedspotpricemodelandthecorrespondingalgorithmareintroducedinthispaperbasedonthetheoryofoptimalpowerflow.Differentfromthetraditionaleconomicdispatchinthefieldofspotprice,theobjectivefunctionistominimizegenerationcostsbasedonpricingreactivepower.Thenconsideringthecharacteristicsofwindturbines,processingmethodsofwindfarmsinoptimalpowerflowisdiscussed.Finally,thefeasibilityofthemodelandthealgorithmisverifiedthroughthesimulationresultsofIEEE30system.
简介:Strokeisaleadingcauseofdeathanddisabilityinadultsworldwide.Fordecades,theprimaryapproachandgoaloftherapyforstrokehasfocusedonneuroprotection,namelytreatingtheinjuredtissue,withinterventionsdesignedtoreducethevolumeofcerebralinfarction.Enormouseffortinthelaboratoryhasbeendevotedtothedevelopmentof
简介:裂口Hopkinson压力酒吧(SHPB)技术被用来与不同钢纤维内容决定反应粉末水泥(RPC)的动态力量。有不同厚度的脉搏shapers的二种类型被认为减少high-frequency-oscillation效果并且在某个变丑范围上完成将近经常的紧张率。像水泥的材料的压缩力量是hydrostatic-stress-dependent,这被知道,并且明显的动态力量改进来自两个静水力学的压力和紧张的效果评价。以便区分他们,数字方法被用来在RPC的动态压缩强度上计算静水力学的应力,然后真紧张率效果的贡献被决定。另外,动态力量和RPC的失败模式上的钢纤维的效果被讨论。
简介:Thisreviewdealswiththepreparationandapplicationofpolymericsulfinateresinsasreactiveintermediateinsolidphaseorganicsynthesisandseparation.
简介:Manystudiesdemonstratethatconventionalanticancerdrugselevateintracellularlevelofreactiveoxygenspecies(ROS)andalterredox-homeostasisofcancercells.ItiswidelyacceptedthatanticancereffectofthesechemotherapeuticsisduetoinductionofoxidativestressandROS-mediatedapoptosisincancer.Ontheotherhand,theharmfulsideeffectsofconventionalanticancerchemotherapyarealsoduetoincreasedproductionofROSanddisruptionofredox-homeostasisofnormalcellsandtissues.ThisarticledescribesthemechanismsfortriggeringandmodulationofapoptosisthroughROS-dependentandROS-independentpathways.Wetrytoanswerthequestion:'Isitpossibletoinducehighlyspecificapoptosisonlyincancercells,withoutoverproductionofROS,aswellaswithoutharmfuleffectsonnormalcellsandtissues?'Thereviewalsosuggestsanewtherapeuticstrategyforselectivekillingofcancercells,withoutsignificantimpactonviabilityofnormalcellsandtissues,bycombininganticancerdrugswithredox-modulators,affectingspecificsignalingpathwaysandavoidingoxidativestress.
简介:在这个工作,在dodecyl-benzenesulfonic酸和钠碳酸盐之间的使成粒状高在实验室规模被调查砍混合器。包括主要碳酸盐尺寸,文件夹内容,impeller速度,和操作温度,明确的表达参数和过程变量的效果被相关到产品小粒的性质。实验的设计和变化的分析被联合分析试验性的数据,并且结果证明有更少好粒子的更大的小粒尺寸能被采用更高的文件夹内容和更大的钠碳酸盐尺寸获得。impeller的shear力量能广泛地打破oversized小粒。文件夹内容在与二种钠碳酸盐形成的小粒的flowability上施加了形成对照的效果,因为在固体的液体浸透的差别可能。同轴的尺寸分析决定的溶解率证明高文件夹内容对溶解性能,和在亨特之间的关系有益颜色和测试参数被评估。这个工作的结果能在粉末为过程控制和优化被用作可靠指导净化的生产。
简介:ThedisproportionatedphasesofNdHx,Fe2B,anda-FefromNd2Fe14BwereappliedtoprepareNdFeBmagnetsbytwodifferentroutes.Theresultsshowthattherouteofannealinginhorizontalvacuumsinteringfurnacecannotreachthepurposeofcompleterecombinationafterthehotpressingandhotdeformationprocessduetothelackofdehydrogenationchannel.Therouteofapplyinglowpressureof4–25MPaontheas-disproportionatedgreencompactduringthedesorptionrecombinationprocessinsituhotdeformationinasparkplasmasintering(SPS)systemcanobtaincompletelyrecombinedNdFeBmagnetwithgoodanisotropyandmagneticproperties.Themaximummagneticproperties,(BH)max=201kJm-3,Br=1.142TandHcj=469kAm-1,areobtainedafterbeingtreatedfor15minat750°Cunderlowpressure.
简介:四个最初的不连续的Galerkin方法被使用也就是,解决反应运输问题Oden-Babuska-BaumannDG(OBB-DG),非对称的内部penaltyGalerkin(NIPG),对称的内部惩罚Galerkin(SIPG),和不完全的内部penaltyGalerkin(IIPG)。一个统一后验剩余类型错误评价为这些方法明确地被导出。从计算解决方案和给定的数据,明确的评估者能高效地并且直接被计算,它能为改编被用作错误指示物。在参考不同,我们由使用两重性技术而不是inL~2(H~1)在L~2(L~2)标准获得错误评估者标准。
简介:Inthispaper,anovelcopper-basedcatalystforFCCgasolineimprovingtheabilityofremovalthesulfurandavoidingthelossoftheoctanenumberfromolefinsaturationbyreactiveadsorptiondesulfurization(RADS)wasinvestigated.TheseriesofCu/ZnO-Al2O3catalystswerecharacterizedbyX-raypowderdiffraction(XRD),N2adsorptionanalysisandtemperature-programmedreduction(TPR)studies,X-rayphotoelectronspectroscopy(XPS),scanningelectronmicroscope(SEM)andtransmissionelectronmicroscopy(TEM).Theexperimentresultsshowedthatthecatalystshadanoptimumdesulfurizationabilitywithcopperloading6wt%,whichthesulfurcontentsofproductdecreasedlessthan10μg/gandolefincontentsdecreasedfrom16.19%to14.14%forthelongperiodoperation.TheappropriateCuloadingcontentcouldleadtothehighactiveandlowapparentactivationenergy(Ea).Therefore,theCu-basedcatalystmaybecomeanovelcatalystforsecond-generationforreactiveadsorptiondesulfurization,whichachievesthehighdesulfurizationactiveandlowolefinssaturationtosatisfytheupgradingtheproduct.