简介：采用粉末压片法制样,利用鹿鸣矿业钼精矿标准样品建立工作曲线,通过X射线荧光光谱法测定钼精矿中铜。测定结果与国家标准方法的测定值相符,相对标准偏差在0.35%~4.75%之间,可满足日常分析的需要。

简介：采用激光熔覆方法在45#钢基体上制备含TiC质量分数为20%~50%的Fe基TiC复合涂层。分别用扫描电镜（SEM）、能谱仪（EDS）、X线衍射（XRD）、显微硬度计、摩擦磨损机对熔覆层的微观组织、物相、硬度及耐磨性进行研究。结果表明：当TiC质量分数为30%时,涂层组织致密,TiC颗粒分布均匀、部分溶解、尺寸减小;涂层主要是由α-Fe固溶体,FeC,FeB,B4C,B4Si,Cr5B3,TiB以及未溶解的TiC等组成;当TiC质量分数为30%时,熔覆层平均维氏硬度为783.8,磨损率为45#钢基体的1/38。

简介：Aself-developedelectromagneticinduction-heatingdevicewasusedtoinvestigatethevariationinthemicrostructureandpropertiesofX80pipelinesteelintherapidinductiontemperingprocessatdifferentprocessparameters.Theeffectsofthetemperingconditionontoughness,microstructure,sizeanddistributionofprecipitatesofX80pipelinesteelwereobservedusingametallographicmicroscopyandscanningelectronmicroscopy.Comparedwiththesamplespreparedviatraditionaltemperingtechniques,resultsshowthatthesamplespreparedviarapidinductiontemperinghadimprovedperformances.Whentheheatingtemperatureis590℃,ataholdingtimeof90s,itwasfoundthatacicularferritewasrefined,carboniteprecipitationwassmall,andprecipitateswereevenlydistributedinthematrix.Thelow-temperatureimpactenergy,alsoknownastheimpactabsorptionenergy,at-40℃wasfoundtobe430.5Jfortherapidinductiontemperingsamplesand323.2Jforthetraditionallytemperedsample.Thelow-temperatureimpactenergyat-60℃wasfoundtobe351.3Jfortherapidinductiontemperedsampleand312.1Jforthetraditiontemperingsample.

简介：Whitelight-emittingYVO_4：1mol.%Dy~（3＋）,xmol.%Eu~（3＋）phosphorpowderswithordermorphologyandwellcrystallizationwerehydrothermallysynthesizedat180°C.Themicrostructure,white-lightemission,andlight-emittingmechanismofthepowderswerecarefullystudiedusingX-raydiffractometry,scanningelectronmicroscopyandphotoluminescencespectra.TheexcitationandemissionspectraofthephosphorpowdersindicatedthecoexistenceofefficientenergytransferfromEu~（3＋）toDy~（3＋）andinefficientenergytransferfromDy~（3＋）toEu~（3＋）besidestheenergytransferfromVO_4~（3–）toEu~（3＋）.IncreasingtheEu~（~（3＋））concentrationinitiallyenhancedandthenweakenedtheluminescentintensityofDy~（3＋）.Thewhite-lightemissionsofYVO_4：1mol.%Dy~（3＋）,xmol.%Eu~（3＋）phosphorpowderswerebothrelatedtotheenergytransferbetweenVO_4~（3–）andDy~（3＋）/Eu~（3＋）,aswellasbetweenEu~（3＋）andDy~（3＋）.TheinefficientenergytransferfromDy~（3＋）toEu~（3＋）wasfirstfound.