简介:纤维素醚广泛地习惯于臼明确的表达,并且理解在纤维素醚和水泥粘贴之间的相互作用是重要的。英尺红外系列,热分析和SEM被用来在HEMC和HPMC在这篇文章修改的水泥粘贴调查水和产品。结果证明在修改水泥粘贴的水和产品与在未修改的水泥浆糊,而是主要水和产品的那些是最后相同的,例如CH(氢氧化钙),ettringite和C-S-H,比的在修改水泥粘贴显得以后在未修改的水泥浆糊。纤维素醚减少外部产品和增加C-S-H胶化的内部产品。比作未修改的水泥粘贴,没有新产品在现在的实验在修改水泥粘贴被发现。HEMC和HPMC调查几乎在波特兰水泥的水和产品上显示出一样的影响。
简介:Zincwasrecentlysuggestedtobeapotentialcandidatematerialfordegradablecoronaryarterystent.Thecorrosionbehaviorofpurezincexposedtor-SBFupto336hwasinvestigatedbyelectrochemicalmeasurementsandimmersiontests.Themorphologyandchemicalcompositesofthecorrosionproductswereinvestigatedbyscanningelectronmicroscope,grazing-incidenceX-raydiffraction,X-rayphotoelectronspectroscopyandFouriertransforminfraredspectrometer.Theresultsdemonstratethattheinitialcorrosionproductsonthepurezincmainlyconsistofzincoxide/hydroxideandzinc/calciumphosphatecompounds.ThepureZnencountersuniformcorrosionwithanestimatedcorrosionrateof0.02-0.07mmy^-1duringtheimmersion,whichsuggeststhesuitabilityofpureZnforbiomedicalapplications.
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简介:Byanalogueexperimentofexhaustgas,thesensitivecharacteristicsoftitaniatoair/fuelratiowasinvestigated.Theeffectsofsomeimpuri-tiesontheelectricconductivityofTiO2,thedeviationof(A/F)cfrom(A/F)sinnonequilibriumgassystemandtheself-catalyticoxidationofTiO2wereexplainedrespectively.Theeffectsofca-talyst,porosityandthicknessofsensorelementontheresponsetimewasalsoanalyzed.
简介:Samplesofacobalt-basedalloythatunderwentasurfacetreatmentwereevaluated.Thesamples,whichwereobtainedbycastingalloyASTMF75,weregroundandpolishedononesideuntilamirrorfinishwasobtained.Thesampleswereencapsulatedinwollastonite(W)usinguniaxialpressure,treatedat1220℃for1handsubsequentlytemperedinwater.Thecharacterisationofthesampleindicatedthatpartoftheceramicencapsulatingmaterialwasmechanicallyincorporatedonthemetallicsurfacebygrowthoftheoxidelayerofthealloy.Afterthermaltreatment,aseriesofspecimensweresubmergedinasolutionwith5-foldsimulatedbodyfluid(5SBF)for3,5and21days.Characterisationbyscanningelectronmicroscopy(SEM),energydispersivespectroscopy(EDS)andX-raydiffraction(XRD)indicatednucleationandgrowthofahomogenouslayerofapatite,beginningonthethirddaywhenthesamplewassubmerged.
简介:Thestatusandthevariationofelectricalresistanceofimpactedcarbonfiber/epoxy-matrixcompositeswerestudiedbyultrasonicF-scanandelectricalresistancemeasurementTheexperimentalresultsshowsthatimpactdamageenergythresholdvalueofcarbonfabric/epoxy-matrixcompositescandeterminebyusingultrasonicF-scan.Whentheimpactenergyexceedsthethresholdvalue,damageisgeneratedincomposites.Electricalresistanceofimpactedcompositesischangedowingtothecontactofeachcarbonfiberunitincomposites,whichcauseachangeoftheseries-parallelinconductors.Theveracityofdetectingimpactdamageincompositescanbeimprovedinthiscase.
简介:以KF、SbCl3和SnCl2为原料配制乙醇溶胶,通过在Ti基底上涂胶、干燥、预热处理和煅烧等工艺制备出了F—Sb-SnO2/Ti复合电极。以F—Sb—SnO2/Wi复合电极为阳极,镍片为阴极,施加恒电压观测甲基橙电解液的脱色变化,在正交设计试验基础上,考察溶胶涂层数、煅烧温度、掺杂F离子的浓度等因素对甲基橙降解率的影响,结果表明,固定电解参数电压3V,甲基橙浓度50mg/L,添加荆h(Ⅲ)浓度110mg/L,溶液pH=l,优化的溶胶涂层数9,煅烧温度为773K,溶胶中维持Sn/Sb摩尔比9/1时,优化的KF掺杂摩尔比为0.5时,电解75min,甲基橙的降解率达93%。