简介：PureAl2O3-2SiO2powderswerepreparedbysol-gelandcoprecipitationmethods,andtheiralkaliactivationreactivitieswerecompared.Thealkali-activationreactivityofthepowderpreparedbythesol-gelmethodwashigherthanthatofthepowderpreparedbythecoprecipitationmethod.Thepowderswereinvestigatedby27AIand29Simagic-anglespinningnuclearmagneticresonancespectroscopy（MASNMR）tounderstandtherelationshipbetweentheirstructureandalkali-activationreactivity.The27AlMASNMRdatashowedthatthefive-coordinateAIcontentofthepowderpreparedbythesol-gelmethodwashigherthanthatofthepowderpreparedbycoprecipitation.Thehighercontentoffive-coordinateAlcorrespondedtohigheralkali-activationreactivity.The29SiMASNMRdatashowedthatforthepowderpreparedbythesol-gelmethod,siliconwasreplacedbyaluminumatsecondarycoordinationsitesofthecentralSiatomsduringcalcination.However,forthepowderpreparedbysingle-batchcoprecipitation,themainchangewasfromalowdegreeofpolycondensationtoahighdegreeofpolycondensation.

简介：Inthealloywithsolutecontenthigherthanthelimitingsolubility,thesoluteatomsthathavefailedtodissolvewillprecipitatefromthesolidsolutionandformprecipitations.Inthisstudy,thePortevin-LeChatelier(PLC)effectsinannealed5456and5052aluminumalloyswithdifferentprecipitationcontentshavebeeninvestigatedunderdifferentappliedstrainrates.TheresultssuggestthatprecipitationshavesignificanteffectonthePLCeffectandthemoretheprecipitationsare,thegreaterthe...

简介：Acleanmethodforpreparinglayereddoublehydroxides(LDHs)hasbeendeveloped,featuredbyusingthehydroxidesoftwodifferentmetalsasstartingmaterialsbyatom-economicreactions.Thereactionswerecarriedoutunderhydrothermalconditionsineitherahighpressureautoclaveoramicrowavedigester.Thecompositions,structuralparametersandthermalbehavioroftheresultingLDHsareverysimilartothoseofmaterialsproducedbyusingtheseparatenucleationandagingsteps(SNAS)method.Themajoradvantageofthenewmethodisthatnoby-productisproduced,sothatfiltrationandwashingprocessesareunnecessary.Theconsequentreductioninwaterconsumptionisbeneficialtotheenvironment.

简介：平台漂移误差测试和标定是保证惯性系统精度最基本的措施之一,应用于武器载体特别是战术弹时,要求尽量延长标定周期.在长期存储过程中,陀螺、加速度计等惯性元件测量轴的安装精度会因安装应力和自重应力作用而有损失,使平台漂移模型失真.理论分析表明,复合材料技术可大大减小此类误差,从而可通过长期保持惯导系统机械零位精度来延长平台标定周期.

简介：密度功能的理论(DFT)学习被执行了为[Znn?1Al(OH2)n+6(哦)2n?2]3+(n=36)并且[Znn?1Al(OH2)2n?2(哦)2n?2]3+(n=7)簇，它包括象brucite一样格子的基本结构的信息在范围与Zn/Al臼齿的比率(R)Zn/Al分层的双氢氧化物(LDH)组织26，以便在二进制Zn/AlLDH的结构和稳定性上理解Zn/Al比率的效果。基于几何参数的系统的计算和簇模型的形成精力，Zn2+和Al3+阳离子用不同R价值在象brucite一样结构同态地代替Mg2+是可能的，这被发现，在簇和单位房间参数的微观结构导致差别一ofZn/AlLDH。几何学的分析并且在三价的Al3+或二价的Zn2+阳离子附近结合表明Al3+在当时，决定微观结构性质，形成和相应ZnRAl簇的结合的稳定性比Zn2+起一个更重要的作用R<5，当Zn2+的影响在R5的情况中成为主导的因素时。这些调查结果在对实验的好同意。这个工作提供阳离子的作文怎么影响包含Zn二进制LDH层的微观结构和稳定性的详细电子水平的理解。

简介：一本文提出了用ＥＰＬＤ芯片实现高分辨率的双边沿鉴频鉴相器，从而解决了锁相伺服系统的高精度问题。

简介：TiO2nanoparticlesweresynthesizedbyahomogeneouscontrolledprecipitationmethodusingindustrialtitaniumsulfate(Ti(SO4)2).TheobtainedpowderswerecharacterizedbyX-raydiffraction(XRD),transmissionelectronmicroscope(TEM),Fouriertransforminfraredspectroscopy(FTIR)andICPplasmaspectrometer.EDTAwasusedascomplexingagenttoimprovethepurityandtheformationofTiO2nanoparticles.Experimentalresultsindicatedthatthehigh-purityTiO2nanoparticleswere20nminmeansizeandnearlymonodispersed.

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简介：BSTOdielectricceramicwaspreparedfromSrTiO3andBaTiO3powderssynthesizedbyhydrothermalmethod,aswellasfromBa0.6Sr0.4TiO3powdersynthesizedbyconventionalsolid-statereaction.Theformercanbesinteredatarelativelylowtemperatureof1120℃.CharacterizationbySEMshowedthatthegrainshapesofbothceramicsarecubical,thoughthegrainsizeoftheformerismuchsmaller.Dielectricconstantsmeasuredat20℃wereshowntovarywithfrequencyintherangefrom1kHzto2MHzanddcbiasfield,andfurtherthatthedielectriclossoftheformertobelessthan2×10-3inthefrequencyrangeof20kHzto1MHz,muchsmallerthanthatofthelattersample.Fortheformer,temperaturedependenceofdielectricconstantismuchflatterandthereexistsanextendedphasetransitiondiffusioncoveringawidetemperaturerangeofCurietemperatureTc.Thesmallergrainsizeoftheformerdepressesthedcbiaselectricalfielddependenceofdielectricconstant.Thetunabilityis7%underabiasfieldof0.6kV/mmdc.

简介：TiO2@ZrO2@Y2O3:有coremultishell结构的Eu3+合成粒子通过layer-by-layer(LBL)的联合被综合自己组装方法和一个solgel过程。获得的样品与扫描电子被描绘显微镜学(SEM)，传播电子显微镜学(TEM)，X光检查光电子光谱学(XPS)，X光检查衍射(XRD)，和荧光spectrophotometry。结果证明合成粒子有coremultishell结构，球形的形态学，和狭窄的尺寸分布。TiO2核心上的ZrO2层的存在能有效地阻止在TiO2核心和Y2O3壳之间的反应；为在在TiO2@ZrO2@Y2O3的TiO2核心和Y2O3壳之间的反应的温度:Eucoremultishell黄磷能被300提高

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简介：3阶段的水动力学反的使流体化的床为不同液体和煤气的速度用低密度粒子试验性地被学习。水动力学特征学习了包括压力落下，最小的液体和气体使液化速度和阶段劫盗。用床压力坡度决定的最小的液体使液化速度，随气体的增加减少速度。液体劫盗沿着床高度增加的阶段劫盗表演的轴的侧面，而稳固的劫盗减少，击倒床。然而，煤气的劫盗在床上是几乎一致的。

简介：A3-DnonlinearproblemofsupercavitatingflowpastanaxisymmetricbodyatasmallangleofattackisinvestigatedbymeansoftheperturbationmethodandFourier-cosine-expansionmethod.Thefirstthreeorderperturbationequationsarederivedindetailandsolvednumericallyusingtheboundaryintegralequationmethodanditerativetechniques.Computationalresultsofthehydrodynamiccharacteristicsandcavityshapesofeachorderarepresentedfornonaxisymmetricsupercavitatingflowpastconeswithvariousapex-anglesatdiffer-entcavitationnumbers.Thenumericalresultsarefoundingoodagreementwithexperimentaldata.

简介：文章通过对EFM（effectivefieldmodeling）模型进行简化,消除了原模型的非守恒性项和非双曲性特性项,发展了一种基于密度的气液两相流模拟方法：ρ-VOF方法.利用体积分数信息对控制单元内的自由界面进行重构,得到了控制单元内流体的空间分布,并采用AUSM^＋-up格式获得考虑气液流体接触间断信息的对流通量.新方法可统一处理激波间断和接触间断的相互作用,保持自由界面的尖锐性,并且其计算量与自由界面的空间复杂度无关.最后,数值模拟了液体激波管气液激波管和气体激波跨二维液滴传播等问题,并与文献结果进行对比,验证了本方法在气液两相流模拟中的准确性.

简介：Soilconsolidationwouldinducevariationsofitstransportcoefficientssuchashydraulicconductivityanddiffusioncoefficient.Thispaperpresentsastudyoftheinfluenceofbarrierconsolidationontransportcoefficients,anda3Dtransportmodelbasedonmixturetheoryisproposedfordescribingthelinersthatinvolvecirculardefectsinthegeomembrane.TheelastoplasticALPHAmodelisrevisedbyusingthespatiallymobilizedplane(SMP)criterionforsimulatingthedeformationofthesoils.Then,the3Dmodelcouplingthenonlinearconsolidationandcontaminantadvection-diffusionissolvedusingthefiniteelementsoftwareABAQUS.Theresultsshowthattheimportanceofreducingthedefectsizeinthegeomembraneandthelinerporositytocontrolthecontaminantconcentrationincrease.

简介：TheIsodynetechniquebasedonthescatteredlightscanningfromathinlaserbeamcanbeusedtoobtaintheinformationinsidetheloadedobjectintheroomtemperaturenondestructively,soitisaverypowerfultechniquein3Dstressanalysis.Theproblemsarehowtointerprettheinformationandhowtogetsufficientinformationfromthefewinterferencefringe.Birefringencephaseshifttechniquecandistinguishthefringeordersautomaticallyandenrichtheinformationin256graylevelsbetweenmaximandminimlightintensity.InthepapertheIsodynebirefringencephaseshiftmethodwithanobliqueincidenceandequilibriumequationispresented,bywhichthe3DstressesinthemiddleplaneofaplatewithUshapenotchareseparatedsuccessfully.

简介：Basedonthegeneralconservationlawsincontinuummechanics,theEulerianandLagrangiandescriptionsofthejumpconditionsofshockwavesin3-dimensionalsolidswerepresentedrespectively.Theimplicationofthejumpconditionsandtheirrelationsbetweeneachother,particularlytherelationbetweenthemassconservationandthedisplacementcontinuity,werediscussed.Meanwhiletheshockwaveresponsecurvesin3-dimensionalsolids,i.e.theHugoniotcurveswereanalysed,whichprovidethefoundationforstudyingthecouplingeffectsofshockwavesin3-dimensionalsolids.

简介：The1/3subharmonicsolutionfortheDuffing'sequationisinvestigatedbyusingthemethodsofharmonicbalanceandnumericalintegration.Thesensitivityofparametervariationforthetransientprocessandthetransientprocessfortheperturbanceinitialconditionsarestudied.Overandabove,theprecisionofnumericalintegrationmethodisdiscussedandthenumericalintegrationmethodiscomparedwiththeharmonicbalancemethod.Finally,asymptoticalstabilityofthepuresubharmonicoscillationselementisinspected.

简介：Uniformlysizedα-Fe2O3hexagonalplateletsweresynthesizedbyahydrothermalprocessusingFe(OH)3suspensionandlargeamountofNaOH.ThereactionproductswerecharacterizedbyX-raydiffraction(XRD),scanningelectronmicroscopy(SEM),transmissionelectronmicroscopy(TEM),selectedareaelectrondiffraction(SAED),andavibratingsamplemagnetometer(VSM).Theresultsshowthatthehexagonalplateletsarefine,monodisperseandconsistingofsingle-crystals.Themagnetichysteresis(M-H)curveofthesamplesmeasuredatroomtemperatureindicatesthattheα-Fe2O3micro-plateletsexhibitferromagneticbehaviorswithrelativelylowcoercivity.

简介：Becausemostpiezoelectricdeviceshaveinterfaceswithfluidinengineering,itisvaluabletostudythecoupledfieldbetweenfluidandpiezoelectricmedia.Asthefundamentalproblem,the3DGreen'sfunctionsforpointforcesandpointchargeloadedinthefluidandpiezoelectricbimaterialsarestudiedinthispaper.Basedonthe3Dgeneralsolutionsexpressedbyharmonicfunctions,weconstructedthesuitableharmonicfunctionswithundeterminedconstantsatfirst.Then,thecouplefieldinthefluidandpiezoelectricbimaterialscanbederivedbysubstitutionofharmonicfunctionsintogeneralsolutions.Theseconstantscanbeobtainedbyvirtueofthecompatibility,boundary,andequilibriumconditions.Atlast,thecharacteristicsoftheelectromechanicalcoupledfieldsareshownbynumericalresults.