Synthesis of 3,3,5,5-tetrabenzyl-l,2,4-trithiol and 1,2-dis（ 1,3-arylpropan-2-yl）disul fane-中国期刊网

摘要 Novelsulfur-containingcompounds(3a–3c,4a–4c)wereobtainedinethanolwith1,3-diphenyl-2-propanoneasthestartingmaterial.Theadvantagesofthisprocedureweremildreactionconditions,simpleprotocol,andhighyields.ThestructuresoftheproductswerecharacterizedbyIR,1HNMR,MSandelementaryanalysis.Thecrystalofthenewcompound4abelongstomonoclinic,spacegroupC2witha=18.727(3),b=6.5179(9),c=13.7576(18),b=131.0610(10)°,V=1266.2(3)A3,Z=2,Dc=2.136g/cm3,μ=1.078mm-1,F(000)=843,R=0.0490andwR=0.1247for3211observedreflectionwithI>2δ(I).X-rayanalysisrevealsthatthemoleculeisnotsymmetrical,themolecularstructureisstabilizedbyweakp–pstackinginteractions,andnoclassicalhydrogenbondscanbeobserved.

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Synthesis of 3,3,5,5-tetrabenzyl-l,2,4-trithiol and 1,2-dis（ 1,3-arylpropan-2-yl）disul fane

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Synthesis of 3,3,5,5-tetrabenzyl-l,2,4-trithiol and 1,2-dis（ 1,3-arylpropan-2-yl）disul fane

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